HRID64116
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
The compound was prepared from the compound of Example 99 using the procedures of Example 100 and cyclopropane sulfonyl chloride. 1H NMR, 300 MHz: (DMSO-d6): δ 10.3 (s, 1H), 8.8 (s, 1H), 8.61 (s, 1H), 8.25 (s, 1H), 7.91 (d, 1H), 7.78 (d, 1H), 7.69 (s, 1H), 7.46-7.43 (m, 4H), 6.34 (t, 2H), 4.12 (s, 3H), 2.94 (m, 1H), 1.04-1.02 (m, 4H); LC-MS (ESI): Calculated mass: 459.52; Observed mass: 460.1 [M+H]+ (rt: 1.22 min).
WORKUP
后处理
- custom460.1 [M+H]+ (rt: 1.22 min)