Thionyl Chloride → HCID 66754456, compound

HRID 641357Notes

Reaction equation

HRID 641357 reaction equation
O[CH2:2][C:3]1[N:4]=[C:5]2[C:10](=[C:11]3[C:16]=1[CH:15]=[CH:14][CH:13]=[CH:12]3)[CH2:9][CH2:8][CH2:7][CH2:6]2.S(Cl)([Cl:19])=O>C(Cl)Cl>[ClH:19].[Cl:19][CH2:2][C:3]1[N:4]=[C:5]2[C:10](=[C:11]3[C:16]=1[CH:15]=[CH:14][CH:13]=[CH:12]3)[CH2:9][CH2:8][CH2:7][CH2:6]2

Participants

4

Reactant 2

HCID 24386Thionyl ChlorideHCID 66754357HCID 66754357, compound

Product 1

HCID 66754456HCID 66754456, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Prepared by treating 110 mg of 6-hydroxymethyl-1,2,3,4-tetrahydro-phenanthridine with 60 μl of thionyl chloride in 2.5 ml methylene chloride at 0° C. to ambient temperature.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-bef9ac2adef641d89e09528197319a7f
Source dataset
uspto-grants-2010_04
Patent number
US07696212B2

Reaction notes

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