HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 62239198, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 68578245 | HCID 68578245 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 62239198 | HCID 62239198 | — |
Reaction Steps
A solution of 2.32 g (11.1 mmol) of the ester from step C in 25 ml of ethanol is reduced by portion wise addition of 2.09 g (55.4 mmol) of sodium borohydride. HPLC analysis after stirring at r.t. for 12 hours shows complete reaction. The mixture is diluted with methanol and extracted with ethyl acetate/water to yield a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07696216B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-30232e33116f4bd3902e66c4e0c504e5 |
| Source note | uspto-grants-2010_04 |