関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 6-Methyl-3-(2H-1,2,3-triazol-2-yl)picolinonitrile | HCID 68281582 | — |
| 生成物 | 6-methyl-3-(2H-1,2,3-triazol-2-yl)picolinic acid | HCID 59363733 | — |
反応手順
To a solution of the title compound of Step A (730 mg, 4 mmol) in EtOH (10 mL) was added 4 N NaOH (1 mL, 4 mmol). The mixture was heated at 100° C. for 24 h. The reaction mixture was concentrated in vacuo to a white solid which was used without further purification in subsequent steps. MS (ESI) mass calcd. for C9H8N4O2, 204.1. m/z found 205.1 [M+H]+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US09447117B2 |
|---|
| 出典データセット | uspto-grants-2016_09 |
|---|
| ORD ID | ord-a6fc142842d84e73accb3ea2282c7394 |
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| 出典メモ | uspto-grants-2016_09 |
|---|
