HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 64225Generated: October 29, 2026
Thionyl Chloride → 3-(1-Cyanoethyl)benzoyl chloride
https://huagongshe.com/reaction/64225
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-(1-Cyanoethyl)benzoic acid | HCID 98370 | — |
| Product | 3-(1-Cyanoethyl)benzoyl chloride | HCID 3016393 | — |
Reaction Steps
Thionyl chloride (10 mL) was added at 0° C. to 3-(l-cyanoethyl)benzoic acid (12, 500 mg, 2.85 mmol). The reaction mixture was heated at 80° C. for 2 h. The excess thionyl chloride was removed to give 3-(l-cyanoethyl)benzoyl chloride, which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09447134B2 |
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| Source dataset | uspto-grants-2016_09 |
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| ORD ID | ord-8877b751d591410e9acb89acc69b4fd4 |
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| Source note | uspto-grants-2016_09 |
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