HuagongsheHuagongshe Chemistry Print Report · For research reference only
ethyl 2-methyl-1H-indole-3-carboxylate → 2-Methyl-1-phenyl-1H-indole-3-carboxylic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | ethyl 2-methyl-1H-indole-3-carboxylate | HCID 4072358 | — |
| Reactant | Ethyl 2-methyl-1-phenyl-1H-pyrrole-3-carboxylate | HCID 15272135 | — |
| Product | 2-Methyl-1-phenyl-1H-indole-3-carboxylic acid ethyl ester | HCID 15953410 | — |
Reaction Steps
Prepared in analogy to that of 2-methyl-1-phenyl-1H-pyrrole-3-carboxylic acid ethyl ester from 2-Methyl-1H-indole-3-carboxylic acid ethyl ester. The title compound, 1H NMR (200 MHz, CDCl3): δ (ppm)=8.15 (d, 1H, J=7.4 Hz), 7.6-6.9 (m, 8H), 4.43 (q, 2H, J=7.4 Hz), 2.59 (s, 3H), 1.47 (t, 3H, J=7.4 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07696223B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-077312ff0a8743a7abee8be20c68df7b |
| Source note | uspto-grants-2010_04 |