HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 86617365, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 68426685 | HCID 68426685 | — |
| Catalyst | Benzoyl Peroxide | HCID 7187 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 86617365 | HCID 86617365 | 117.1% |
Reaction Steps
A mixture of 4-hydroxy-9-methyl-9H-beta-carboline-3-carboxylic acid ethyl ester (511 mg), NBS (354 mg), and BzOOBz (12.7 mg) in carbon tetrachloride (20 mL) was refluxed for 25 min; then cooled, solvents were removed, the residue was purified with column to give the title compound (773 mg). ESI MS (m/z): 349 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07696223B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-b00b29ae252f4e438f1c5ca1a95bbf3e |
| Source note | uspto-grants-2010_04 |