HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isonicotinic Acid → N-(3-nitrophenyl)isonicotinamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isonicotinic Acid | HCID 5922 | — |
| Reactant | 3-Nitroaniline | HCID 7423 | — |
| Product | N-(3-nitrophenyl)isonicotinamide | HCID 790430 | — |
Reaction Steps
The general procedure for 8 was followed using 3-nitro aniline 31 and isonicotinic acid to afforded (68%) as a yellow solid. 1H NMR (DMSO-d6, 400 MHz) δ 7.67-7.71 (m, 1H), 7.89-7.91 (m, 2H), 8.01 (dd, J, =8.4 Hz, J2=1.6 Hz, 1H), 8.19 (dd, J, =8 Hz, J2=1.6 Hz, 1H), 8.79-8.83 (m, 3H), 10.9 (NH, s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09447134B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-1c2729b44194419fb2ac3e8fbe0ef614 |
| Source note | uspto-grants-2016_09 |