HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylacetamide → HCID 68428040, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylacetamide | HCID 31374 | — |
| Reactant | HCID 87451629 | HCID 87451629 | — |
| Catalyst | Zinc cyanide (Zn(CN)2) | HCID 11186 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Catalyst | Ferrocene-1,1'-bis-(diphenylphosphine) | HCID 635956 | — |
| Catalyst | Bis(dibenzylideneacetone)palladium | HCID 9811564 | — |
| Product | HCID 68428040 | HCID 68428040 | — |
Reaction Steps
Prepared in analogy to that of Example 111(a) from 2,3,7-trichloro-4-hydroxy-1-phenyl-1H-pyrrolo[2,3-c]pyridine-5-carboxylic acid ethyl ester, Zn(CN)2, Zn dust, Pd2(dba)3, and dppf in DMA (N,N-dimethylacetamide). The title compound, ESI MS (m/z): 376 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07696223B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-8ce7e373586e4cb4a96d1ede8ff4ed75 |
| Source note | uspto-grants-2010_04 |