Tributylphenyltin → HCID 68426698, compound

HRID 642571Notes

Reaction equation

[CH2:1]([O:3][C:4]([C:6]1[N:11]=[C:10](Br)[C:9]2[N:13]=[C:14]([CH3:16])[S:15][C:8]=2[C:7]=1[OH:17])=[O:5])[CH3:2].C([Sn](CCCC)(CCCC)[C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1)CCC>>[CH2:1]([O:3][C:4]([C:6]1[N:11]=[C:10]([C:23]2[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=2)[C:9]2[N:13]=[C:14]([CH3:16])[S:15][C:8]=2[C:7]=1[OH:17])=[O:5])[CH3:2]

Participants

Reactant 2

HCID 607632Tributylphenyltin

HCID 86617378HCID 86617378, compound

Product 1

HCID 68426698HCID 68426698, compound

Procedure

The title compound was prepared from 4-Bromo-7-hydroxy-2-methyl-thiazolo[4,5-c]pyridine-6-carboxylic acid ethyl ester and tributylphenyl tin under conditions analogous to the experimental procedure found in example 169(a). MS (ESI+): m/z 315.1 (M+1).

Sources & evidence

ORD record: ord-6d5b00ecd9124ebba40c4dc36d9fe3a4
Source dataset: uspto-grants-2010_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07696223B2

Reaction notes

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