7-Chloro-1,2,3,4-tetrahydronaphthalen-1-one → 6-Chloro-4-methyl-1,2-dihydronaphthalene

Participants

Role	Name	HCID	Charge
Reactant	7-Chloro-1,2,3,4-tetrahydronaphthalen-1-one	HCID 256677	—
Reactant	HCID 178418373	HCID 178418373	—
Product	6-Chloro-4-methyl-1,2-dihydronaphthalene	HCID 68579260	—

Reaction Steps

Using general procedure A (Exp. 1.1), 7-chloro-3,4-dihydro-2H-naphthalen-1-one (Lit. 13) was reacted with MeMgI to give 6-chloro-4-methyl-1,2-dihydro-naphthalene as a yellow oil. MS: 178.0 ([M]+).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07696240B2
Source dataset	uspto-grants-2010_04
ORD ID	ord-64fd84edc471490488d580414151992d
Source note	uspto-grants-2010_04