4-Amino-4'-cyanobiphenyl → HCID 24760123, compound

HRID 642810Notes

Reaction equation

HRID 642810 reaction equation
C[O:2][C:3](=[O:22])[CH2:4][CH2:5][NH:6][C:7](=[O:21])[C:8]1[CH:13]=[CH:12][C:11]([C:14](=O)[CH2:15][CH2:16][CH2:17][CH2:18][CH3:19])=[CH:10][CH:9]=1.[NH2:23][C:24]1[CH:29]=[CH:28][C:27]([C:30]2[CH:35]=[CH:34][C:33]([C:36]#[N:37])=[CH:32][CH:31]=2)=[CH:26][CH:25]=1>>[C:36]([C:33]1[CH:32]=[CH:31][C:30]([C:27]2[CH:28]=[CH:29][C:24]([NH:23][CH:14]([C:11]3[CH:12]=[CH:13][C:8]([C:7]([NH:6][CH2:5][CH2:4][C:3]([OH:2])=[O:22])=[O:21])=[CH:9][CH:10]=3)[CH2:15][CH2:16][CH2:17][CH2:18][CH3:19])=[CH:25][CH:26]=2)=[CH:35][CH:34]=1)#[N:37]

Participants

3

Reactant 2

HCID 971934-Amino-4'-cyanobiphenylHCID 67484898HCID 67484898, compound

Product 1

HCID 24760123HCID 24760123, compound

Procedure

The title compound is prepared by the general method exemplified in Example 1 using 3-(4-hexanoyl-benzoylamino)-propionic acid methyl ester (Preparation 5) and 4′-amino-biphenyl-4-carbonitrile as starting materials. MS (ES): 470.2 [M+H]+.

Sources & evidence

ORD record
ord-f8e710684f2e4fee87d175e183ebe477
Source dataset
uspto-grants-2010_04
Patent number
US07696248B2

Reaction notes

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