HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Cyanide → HCID 68675848, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Cyanide | HCID 9032 | — |
| Reactant | 1-Benzylpiperazine | HCID 75994 | — |
| Reactant | Tetrahydro-4H-pyran-4-one | HCID 121599 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 68675848 | HCID 68675848 | — |
Reaction Steps
6.5 g (99.8 mmol) potassium cyanide were added to a solution of 10.0 g (96.9 mmol) tetrahydropyran-4-one and 17.1 g (97.0 mmol) 1-benzyl-piperazine in 25 mL 4 M HCl and 50 mL water while cooling with ice and the reaction mixture was stirred for 40 h at RT. The precipitate formed was suction filtered, washed with water and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07696209B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-b3ebc06d4ffd472e99b7efc394d819bc |
| Source note | uspto-grants-2010_04 |