反应详情

A suspension of 50 g (0.24 mol) 1-methyl-2-nitro-3-trifluoromethyl-benzene and 4.4 g 10% Pd/C in 300 mL MeOH was hydrogenated at RT and 3000 hPa hydrogen pressure until the theoretical amount of hydrogen had been taken up. The catalyst was filtered off, washed with MeOH and the filtrate was evaporated down. The crude product was further reacted without purification.

1. customwas hydrogenated at RT
2. filtrationThe catalyst was filtered off
3. washwashed with MeOH
4. customthe filtrate was evaporated down
5. customThe crude product was further reacted without purification