HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 64315Generated: October 25, 2026
2-Bromo-1-(3-nitrophenyl)ethan-1-one → HCID 178513496, compound
https://huagongshe.com/reaction/64315
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Bromo-1-(3-nitrophenyl)ethan-1-one | HCID 75213 | — |
| Reactant | HCID 178513497 | HCID 178513497 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178513496 | HCID 178513496 | 11.4% |
Reaction Steps
A mixture of 5-amino-3-(4-phenoxyphenyl)-1H-pyrazole-4-carboxamide (29.4 mg, 0.1 mmol) and 2-bromo-1-(3-nitrophenyl)ethanone (24.4 mg, 0.1 mmol) in EtOH (2 mL) was stirred at 80° C. for 16 hr. The mixture was filtered to afford 5 mg of crude 2-(3-nitrophenyl)-6-(4-phenoxyphenyl)-1H-imidazo[1,2-b]pyrazole-7-carboxamide as a yellow solid. MS (ESI) m/e [M+1]+ 440.0.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09447106B2 |
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| Source dataset | uspto-grants-2016_09 |
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| ORD ID | ord-ee2d4ce594704a0985377a363f5590cf |
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| Source note | uspto-grants-2016_09 |
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