HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 68526126, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | (6-Bromonaphthalen-2-yl)methanol | HCID 13473070 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 68526126 | HCID 68526126 | — |
Reaction Steps
Iodomethane (18.96 g, 133.6 mmol) was added dropwise to ice-cooled mixture of (6-bromo-naphthalen-2-yl)-methanol (15.84 g, 66.8 mmol), sodium hydride 60% in oil (3.84 g, 100.2 mmol), and DMF (100 ml). Water was added and the product was filtered. Yield 16.7 g (99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07700596B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-11b1327df8ff42ba85230a966438592a |
| Source note | uspto-grants-2010_04 |