HCID 15654147, compound → HCID 14344228, compound

Participants

Reaction Steps

In CH2Cl2 was dissolved 8a (1g, 1 eq) and a solution of Pb(OAc)4 (2.03 g, 1.1 eq) in which CH2Cl2 was added dropwise. The resulting solution was stirred 30 min at RT, then hydrolyzed with 1 5 ml of Na2CO3 salt, extracted with CH2Cl2, dried by Na2SO4, evaporated and purified by flash chromatography (SiO2, hexane/AcOEt, 8/2) giving 9a as an orange solid in 37% yield.

Provenance & Evidence