Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | 2-[(Dimethylamino)methylidene]cyclohexane-1,3-dione | HCID 359353 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 59262890 | HCID 59262890 | 69% |
Reaction Steps
A MeOH solution of methylhydrazine 0.046 g (0.01 mol) and 2-dimethylaminomethylene-cyclohexane-1,3-dione 1.67 g (0.01 mol) was stirred at room temperature for 1 h, and then was stirred at 50° C. for 1 h. NMR of crude material indicated the reaction was completed. Work up: The reaction mixture was diluted with ethyl acetate and washed with brine. The organic phase was dried with MgSO4, and the solvent was rotary evaporated. The crude product was filtered through silica gel, and 1.03 g pure product was obtained, the yield is 69%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07700609B2 |
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| Source dataset | uspto-grants-2010_04 |
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| ORD ID | ord-cc82e56264bf4d92b732c5640c11b415 |
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| Source note | uspto-grants-2010_04 |
|---|