HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 22173744, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3,7-Dihydroxy-2-naphthoic Acid | HCID 736299 | — |
| Product | HCID 22173744 | HCID 22173744 | — |
Reaction Steps
To a solution of 3,7-dihydroxynaphthalene-2-carboxylic acid (4.0 g, 19.6 mmol) in MeOH (80 mL) is added thionyl chloride (10 mL, 136 mmol) and it is stirred at RT for 48 h. The solvent is removed and purified to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07700633B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-9a9b388a7bb64698b4ad8e7c0ec669ed |
| Source note | uspto-grants-2010_04 |