HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → 5-[3-Hydroxy-7-(5-hydroxy-4,4-dimethylpentyl)-naphthalen-2-yl]-1,1-dioxo-1,2,5-thiadiazolidin-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Benzoic acid 6-(5-hydroxy-4,4-dimethylpentyl)-3-(1,1,4-trioxo-1,2,5-thiadiazolidin-2-yl)-naphthalen-2-yl ester | HCID 17751433 | — |
| Product | 5-[3-Hydroxy-7-(5-hydroxy-4,4-dimethylpentyl)-naphthalen-2-yl]-1,1-dioxo-1,2,5-thiadiazolidin-3-one | HCID 17751434 | — |
Reaction Steps
The title compound is prepared analogously to Example 11 from benzoic acid 6-(5-hydroxy-4,4-dimethylpentyl)-3-(1,1,4-trioxo-1,2,5-thiadiazolidin-2-yl)-naphthalen-2-yl ester and 1 N NaOH solution to replace KOH: Retention time=1.05 min (Method A); (M−H)−=391.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07700633B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-96fd4d55469e4031a756802bdd11901b |
| Source note | uspto-grants-2010_04 |