Benzenamine, 3,5-bis(trifluoromethyl)- → HCID 23069968, compound

HRID 644419Notes

Reaction equation

HRID 644419 reaction equation
[C:1]([C:6]1[CH:7]=[CH:8][C:9]([O:15][CH3:16])=[C:10]([CH:14]=1)[C:11]([OH:13])=O)(=[O:5])[CH:2]([CH3:4])[CH3:3].[F:17][C:18]([F:31])([F:30])[C:19]1[CH:20]=[C:21]([CH:23]=[C:24]([C:26]([F:29])([F:28])[F:27])[CH:25]=1)[NH2:22]>>[C:1]([C:6]1[CH:7]=[CH:8][C:9]([O:15][CH3:16])=[C:10]([CH:14]=1)[C:11]([NH:22][C:21]1[CH:23]=[C:24]([C:26]([F:27])([F:28])[F:29])[CH:25]=[C:19]([C:18]([F:17])([F:30])[F:31])[CH:20]=1)=[O:13])(=[O:5])[CH:2]([CH3:3])[CH3:4]

Participants

3

Reactant 2

HCID 9480Benzenamine, 3,5-bis(trifluoromethyl)-HCID 17860166HCID 17860166, compound

Product 1

HCID 23069968HCID 23069968, compoundYield 61.4%

Procedure

Using 5-isobutyryl-2-methoxybenzoic acid and 3,5-bis(trifluoromethyl)aniline as the raw materials, the same operation as the Example 16 gave the title compound.

Sources & evidence

ORD record
ord-9506796e951940438c1b9058df12bd50
Source dataset
uspto-grants-2010_04
Patent number
US07700655B2

Reaction notes

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