化工社化工社 化学情報印刷レポート · 研究参考用
2,6-Dinitro-p-cresol → 7-Iodo-5-methyl-1-phenylbenzimidazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,6-Dinitro-p-cresol | HCID 11872 | — |
| 反応物 | 5-Cyano-7-iodo-1-phenylbenzimidazole | HCID 67485627 | — |
| 生成物 | 7-Iodo-5-methyl-1-phenylbenzimidazole | HCID 67485322 | 16% |
反応手順
This was prepared in a similar manner to 5-cyano-7-iodo-1-phenylbenzimidazole, using 4-methyl-2,6-dinitrophenol as starting material to realise the desired product (1.45 g, 16%) m/z, 335.1 (M+H)+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07700638B2 |
| 出典データセット | uspto-grants-2010_04 |
| ORD ID | ord-3e2bec06fd35461f92e6d2cc3e8643e0 |
| 出典メモ | uspto-grants-2010_04 |