HCID 68579385, compound → HCID 87503811, compound

Participants

Reaction Steps

2.8 g (5 mmol) of (E)-3-(3-{2-[3,4-bis(tert-butyldimethylsilanyloxymethyl)phenyl]ethyl}phenyl)pent-2-en-1-ol are dissolved in 50 ml of dichloromethane. 4.3 g (50 mmol) of manganese dioxide are added, and the reaction medium is stirred for 12 hours, then filtered and concentrated under reduced pressure. The desired product is obtained in the form of yellow oil (m=2.8 g; Y=100%).

Provenance & Evidence