HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-[3-(tert-Butyldimethylsilanyloxy)phenyl]propan-1-ol → 1-[3-(tert-Butyldimethylsilanyloxy)phenyl]propan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-[3-(tert-Butyldimethylsilanyloxy)phenyl]propan-1-ol | HCID 68579551 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Product | 1-[3-(tert-Butyldimethylsilanyloxy)phenyl]propan-1-one | HCID 15049953 | — |
Reaction Steps
In a manner analogous to example 1j, by reaction of 45 g (0.17 mol) of 1-[3-(tert-butyldimethylsilanyloxy)phenyl]propan-1-ol with (148 g, 1.7 mol) of manganese dioxide. A yellow oil is obtained (m=45 g, Y=100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07700657B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-51472ba040744b56ad5abf194f59e5cb |
| Source note | uspto-grants-2010_04 |