Tetrabutylammonium Fluoride → HCID 59263690, compound

Participants

Reaction Steps

In a manner analogous to example 2m, by reaction of 1 g (1.4 mmol) of (E)-6-(3-{2-[3,4-bis(tert-butyldimethylsilanyloxymethyl)phenyl]ethyl}-phenyl)-1,1,1-trifluoro-2-trifluoromethyloct-5-en-3-yn-2-ol with 3.3 ml (3.3 mmol) of a 1.0 M solution of tetrabutylammonium fluoride. A yellowish solid is obtained (m.p.=123° C.; m=570 mg; Y=84%).

Provenance & Evidence