Sodium Methoxide → HCID 11652651, compound

Participants

Reaction Steps

Compound 4 (10 mg, 0.023 mmol) was dissolved in methanol (1.5 mL) and stirred over night at room temperature with sodium methoxide solution 1M (0.5 mL). The mixture was neutralized with Duolite™ resin, filtered and concentrated in vacuo. The residue was purified by column chromatography (SiO2, CH2Cl2:MeOH 25:1) to give 10 (5 mg, 70%).

Provenance & Evidence