HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isatin → HCID 66642639, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isatin | HCID 7054 | — |
| Reactant | 1-Bromopentane | HCID 8057 | — |
| Reactant | 4-Bromoindole | HCID 676494 | — |
| Reactant | Benzyl 3-Bromopropyl Ether | HCID 2776064 | — |
| Product | HCID 66642639 | HCID 66642639 | — |
Reaction Steps
Following the procedure as described in PREPARATION 1A, and making non-critical variations to replace 4-bromoindole with isatin, and 1-bromopentane with benzyl 3-bromopropyl ether, the title compound was obtained (95%) as a pale yellow syrup: 1H NMR (300 MHz, CDCl3) δ 7.57-6.92 (m, 9H), 4.50 (s, 2H), 3.84 (t, 2H), 3.54 (t, 2H), 2.03-1.94 (m, 2H); MS (ES+) m/z 296.3 (M+1), 318.3 (M+23).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07700641B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-94b3e6dece6946e2b2e134c15afcff93 |
| Source note | uspto-grants-2010_04 |