Sesamol → HCID 12004407, compound

HRID 645125Notes

Reaction equation

HRID 645125 reaction equation
[CH:1]1([CH2:4][CH2:5][N:6]2[C:14]3[C:9](=[CH:10][CH:11]=[CH:12][CH:13]=3)[C:8](=[O:15])[C:7]2=[O:16])[CH2:3][CH2:2]1.C(N1C2C(=CC=CC=2)C(=O)C1=O)CCCC.O1C2C=CC(O)=CC=2OC1.[O:43]1[C:47]2[CH:48]=[C:49]([OH:52])[CH:50]=[CH:51][C:46]=2[CH2:45][CH2:44]1>>[OH:15][C:8]1([C:50]2[C:49]([OH:52])=[CH:48][C:47]3[O:43][CH2:44][CH2:45][C:46]=3[CH:51]=2)[C:9]2[C:14](=[CH:13][CH:12]=[CH:11][CH:10]=2)[N:6]([CH2:5][CH2:4][CH2:1][CH2:3][CH3:2])[C:7]1=[O:16]

Participants

5

Reactant 4

HCID 68289SesamolHCID 15810921-Pentyl-1H-indole-2,3-dioneHCID 122365402,3-Dihydro-1-benzofuran-6-olHCID 655965701-(2-cyclopropylethyl)-1H-indole-2,3-dione

Product 1

HCID 12004407HCID 12004407, compound

Procedure

Following the procedure as described in PREPARATION 2B, and making non-critical variations to replace 1-(2-cyclopropylethyl)-1H-indole-2,3-dione with 1-pentyl-1H-indole-2,3-dione, and 1,3-benzodioxol-5-ol with 2,3-dihydrobenzofuran-6-ol, the title compound was obtained (90%) as a white powder: MS (ES+) m/z 376.3 (M+23).

Sources & evidence

ORD record
ord-30901f3f02064dba9fa441de4286121b
Source dataset
uspto-grants-2010_04
Patent number
US07700641B2

Reaction notes

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