HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68615539, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 44136067 | HCID 44136067 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68615539 | HCID 68615539 | — |
Reaction Steps
A solution of 90 mg of 6-(1-ethoxyvinyl)-N-phenylimidazo[1,2-a]pyridine-2-carboxamide in 2 ml of dichloromethane is stirred at 20° C. for 18 hours with 1 ml of 2N hydrochloric acid. The solid is filtered off, washed with dichloromethane and then with diisopropyl ether, and dried to give 67 mg of 6-acetyl-N-phenylimidazo[1,2-a]pyridine-2-carboxamide hydrochloride (1:1) in the form of a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07704989B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-e4dfa49165bb4fea9f3f7551c9f65927 |
| Source note | uspto-grants-2010_04 |