HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 135856747, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 135856741 | HCID 135856741 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 135856747 | HCID 135856747 | — |
Reaction Steps
22 mg (0.045 mmol) of 5-methyl-2-[5-(4-methyl-piperazine-1-sulphonyl)-2-propoxy-phenyl]-7-propyl-3H-imidazo[5,1-f][1,2,4]triazin-4-one are dissolved in 2 ml of ether and 1 ml of dichloromethane and admixed with 0.1 ml of a 1M solution of HCl in ether. After 20 minutes, the precipitate is filtered off with suction and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07704999B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-efc9aba1ee0d4b468c1a133d4c20324c |
| Source note | uspto-grants-2010_04 |