2-Phenoxynicotinonitrile → HCID 16794656, compound

HRID 645529Notes

Reaction equation

HRID 645529 reaction equation
[O:1]([C:8]1[N:15]=[CH:14][CH:13]=[CH:12][C:9]=1[C:10]#[N:11])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>[Ni]>[O:1]([C:8]1[C:9]([CH2:10][NH2:11])=[CH:12][CH:13]=[CH:14][N:15]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 1

HCID 842422-Phenoxynicotinonitrile

Product 1

HCID 16794656HCID 16794656, compound

Reagents, catalysts & solvents 1

HCID 935NickelCatalyst

Procedure

2-phenoxynicotinonitrile and Raney/nickel were processed according to the Example 78B to afford the title compound. MS (ESI+) m/z 201 (M+H)+

Sources & evidence

ORD record
ord-83faf1dff8db46c48bf95ece8b9e0c66
Source dataset
uspto-grants-2010_04
Patent number
US07704997B1

Reaction notes

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