2-Methyl-5-hydroxypyridine → HCID 62074621, compound

HRID 645533Notes

Reaction equation

HRID 645533 reaction equation
[OH:1][C:2]1[CH:3]=[CH:4][C:5]([CH3:8])=[N:6][CH:7]=1.F[C:10]1[N:17]=[CH:16][CH:15]=[CH:14][C:11]=1[C:12]#[N:13]>>[CH3:8][C:5]1[N:6]=[CH:7][C:2]([O:1][C:10]2[N:17]=[CH:16][CH:15]=[CH:14][C:11]=2[C:12]#[N:13])=[CH:3][CH:4]=1

Participants

3

Procedure

5-hydroxy-2-methylpyridine and 2-fluoronicotinonitrile were processed according to the method of Example 128B to provide the product. MS (ESI+) m/z 212 (M+H)+;

Workup

  1. customto provide the product

Sources & evidence

ORD record
ord-574e468c2baa4aa58ce1b438736ff472
Source dataset
uspto-grants-2010_04
Patent number
US07704997B1

Reaction notes

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