2-Chloro-3-pyridinol → HCID 86082289, compound

HRID 645554Notes

Reaction equation

HRID 645554 reaction equation
F[C:2]1[N:9]=[CH:8][CH:7]=[CH:6][C:3]=1[C:4]#[N:5].[Cl:10][C:11]1[C:16]([OH:17])=[CH:15][CH:14]=[CH:13][N:12]=1>>[Cl:10][C:11]1[C:16]([O:17][C:2]2[N:9]=[CH:8][CH:7]=[CH:6][C:3]=2[C:4]#[N:5])=[CH:15][CH:14]=[CH:13][N:12]=1

Participants

3

Reactant 2

HCID 811362-Chloro-3-pyridinolHCID 27832543-Cyano-2-fluoropyridine

Product 1

HCID 86082289HCID 86082289, compound

Procedure

2-Fluoro-nicotinonitrile was reacted with 2-chloro-pyridin-3-ol according to the method of Example 85A to provide the title compound. MS (DCI/NH3) m/z 232 (M)+, 234 (M+2)+.

Sources & evidence

ORD record
ord-01e5b08fe738431e8821caf7950a0608
Source dataset
uspto-grants-2010_04
Patent number
US07704997B1

Reaction notes

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