Thionyl Chloride → HCID 86082254, compound

HRID 645569Notes

Reaction equation

HRID 645569 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=2[CH2:13]O)[CH:2]=1.S(Cl)(Cl)=O.[N-:19]=[N+:20]=[N-:21].[Na+]>>[N:19]([CH2:13][C:8]1[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=1[C:3]1[CH:2]=[N:1][CH:6]=[CH:5][CH:4]=1)=[N+:20]=[N-:21]

Participants

4

Reactant 3

HCID 24386Thionyl ChlorideHCID 33557Sodium AzideHCID 7537538(2-Pyrid-3-ylphenyl)methanol

Product 1

HCID 86082254HCID 86082254, compound

Procedure

The product of Example 119A, thionyl chloride and sodium azide were processed according to the method of Example 115A to provide the product. MS (ESI+) m/z 211 (M+H)+.

Workup

  1. customto provide the product

Sources & evidence

ORD record
ord-bc9df79daa9042e797ffcc30313b18ec
Source dataset
uspto-grants-2010_04
Patent number
US07704997B1

Reaction notes

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