HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylboronic Acid → 2-Phenyl-3-(1-pyrrolidinyl)-4-pyridinecarbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | HCID 86082298 | HCID 86082298 | — |
| Product | 2-Phenyl-3-(1-pyrrolidinyl)-4-pyridinecarbonitrile | HCID 68582482 | 66% |
Reaction Steps
Prepared in 66% yield from the product of Example 181A and phenylboronic acid according to the procedure described for Example 153A. MS (ESI+) m/z 249.8 (M+H)+; 1H NMR (DMSO-d6) δ 1.72-1.77 (m, 4H), 3.17-3.21 (m, 4H), 7.38-7.52 (m, 6H), 8.14 (d, J=4.7 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07704997B1 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-ccdd4eea52df484fb4de168ed39ba4a7 |
| Source note | uspto-grants-2010_04 |