HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → 2-[(3,6-Dimethyl-1H-indol-2-yl)-phenyl-methyl]-3-hydroxy-4-methyl-4-p-tolyl-cyclobut-2-enone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | 81784-48-7 | HCID 20463626 | — |
| Reactant | 2-Methyl-2-p-tolyl-cyclobutane-1,3-dione | HCID 68581955 | — |
| Product | 2-[(3,6-Dimethyl-1H-indol-2-yl)-phenyl-methyl]-3-hydroxy-4-methyl-4-p-tolyl-cyclobut-2-enone | HCID 24769771 | — |
Reaction Steps
Using general procedure C, 2-methyl-2-p-tolyl-cyclobutane-1,3-dione (from Example 4.1) was reacted with benzaldehyde and 3,6-dimethyl-1H-indole (Lit. 4) to give the title compound as a colorless solid. MS: 420.5 ([M−H]−).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07705034B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-8b407edb9fe64d56a60989af5596f5a3 |
| Source note | uspto-grants-2010_04 |