Benzo[b]thiophen-2-yl(phenyl)methanol → HCID 59264911, compound

HRID 646083Notes

Reaction equation

HRID 646083 reaction equation
[CH3:1][C:2]1([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[C:5](=[O:6])[CH2:4][C:3]1=[O:7].[S:14]1[C:18]([CH:19]([C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)O)=[CH:17][C:16]2[CH:27]=[CH:28][CH:29]=[CH:30][C:15]1=2>>[S:14]1[C:18]([CH:19]([C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)[C:4]2[C:3](=[O:7])[C:2]([CH3:1])([C:8]3[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=3)[C:5]=2[OH:6])=[CH:17][C:16]2[CH:27]=[CH:28][CH:29]=[CH:30][C:15]1=2

Participants

3

Reactant 2

HCID 3311304Benzo[b]thiophen-2-yl(phenyl)methanolHCID 685810272-Methyl-2-phenyl-cyclobutane-1,3-dione

Product 1

HCID 59264911HCID 59264911, compound

Procedure

Using general procedure D, 2-methyl-2-phenyl-cyclobutane-1,3-dione (Lit. 1) was reacted with benzo[b]thiophen-2-yl-phenyl-methanol to give the title compound as a colorless solid. MS: 395.3 ([M−H]−).

Sources & evidence

ORD record
ord-f284d650b958477bb28d520a97b294de
Source dataset
uspto-grants-2010_04
Patent number
US07705034B2

Reaction notes

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