HCID 68580737, compound → HCID 59264920, compound

HRID 646093Notes

Reaction equation

HRID 646093 reaction equation
[CH3:1][C:2]1([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[C:5](=[O:6])[CH2:4][C:3]1=[O:7].[CH3:14][C:15]1[CH:16]=[CH:17][C:18]2[CH:22]=[C:21]([CH:23]([C:25]3[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=3)O)[S:20][C:19]=2[CH:31]=1>>[OH:6][C:5]1[C:2]([CH3:1])([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[C:3](=[O:7])[C:4]=1[CH:23]([C:21]1[S:20][C:19]2[CH:31]=[C:15]([CH3:14])[CH:16]=[CH:17][C:18]=2[CH:22]=1)[C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1

Participants

3

Reactant 2

HCID 68580737HCID 68580737, compoundHCID 685810272-Methyl-2-phenyl-cyclobutane-1,3-dione

Product 1

HCID 59264920HCID 59264920, compound

Procedure

Using general procedure D, 2-methyl-2-phenyl-cyclobutane-1,3-dione (Lit. 1) was reacted with (6-methyl-benzo[b]thiophen-2-yl)-phenyl-methanol to give the title compound as a pale yellow solid. MS: 409.3 ([M−H]−).

Sources & evidence

ORD record
ord-baaec5509fcc451380ec85ac28d0313b
Source dataset
uspto-grants-2010_04
Patent number
US07705034B2

Reaction notes

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