Ethanolamine → HCID 23141455, compound
Reaction equation
[CH3:1][O:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([OH:9])=O)=[CH:5][C:4]=1/[CH:12]=[CH:13]/[C:14]1[CH:19]=[CH:18][C:17]([Br:20])=[CH:16][CH:15]=1.[NH2:21][CH2:22][CH2:23][OH:24]>>[Br:20][C:17]1[CH:18]=[CH:19][C:14](/[CH:13]=[CH:12]/[C:4]2[CH:5]=[C:6]([CH:10]=[CH:11][C:3]=2[O:2][CH3:1])[C:7]([NH:21][CH2:22][CH2:23][OH:24])=[O:9])=[CH:15][CH:16]=1Participants
3
Procedure
The captioned compound was synthesized from 4-methoxy-3-[(E)-2-(4-bromophenyl)vinyl]benzoic acid obtained in step B of Example 2-2-43 and 2-aminoethanol in accordance with the same procedure as in the methods described in step C of Example 1-2-3.
Sources & evidence
- ORD record
- ord-db81d6fbf57d436e83984a79daf5a4e5
- Source dataset
- uspto-grants-2010_04
- Patent number
- US07705053B2
Reaction notes
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