HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 24721357, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 2-Methoxybenzylamine | HCID 81292 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 24721357 | HCID 24721357 | — |
Reaction Steps
A solution of 3.0 mL (0.023 mol) {[2-(methoxy)phenyl]methyl}amine was refluxed in 50 mL 33% HBr in glacial acetic acid until the full deprotection of the starting material. The solvent was evaporated to obtain 4.7 g 2-(aminomethyl)phenol hydrobromide: MS (EI) for C7H9NO: 124.1 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07704995B2 |
| Source dataset | uspto-grants-2010_04 |
| ORD ID | ord-afabc2902f324d2bae04fae5e6a7dc4e |
| Source note | uspto-grants-2010_04 |