Sodium Methoxide → HCID 23715419, compound

HRID 647140Notes

Reaction equation

HRID 647140 reaction equation
[CH:1]1([CH2:6][C:7]2[CH:12]=[CH:11][C:10]([CH:13]([CH3:17])[C:14]([OH:16])=[O:15])=[CH:9][CH:8]=2)[CH2:5][CH2:4][CH2:3][CH2:2]1.C[O-].[Na+:20]>CO>[CH:1]1([CH2:6][C:7]2[CH:8]=[CH:9][C:10]([CH:13]([CH3:17])[C:14]([O-:16])=[O:15])=[CH:11][CH:12]=2)[CH2:2][CH2:3][CH2:4][CH2:5]1.[Na+:20]

Participants

4

Reactant 2

HCID 10942334Sodium MethoxideHCID 19922608HCID 19922608, compound

Product 1

HCID 23715419HCID 23715419, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

50 mg. of 2-(4-cyclopentylmethylphenyl)propionic acid is dissolved in 2 ml. of methanol, titrated with a 3% methanolic sodium methylate solution, concentrated under vacuum, and 50 mg. of sodium 2-(4-cyclopentylmethylphenyl)propionate, m.p. 206° is obtained in this way.

Workup

  1. concentrationconcentrated under vacuum, and 50 mg

Sources & evidence

ORD record
ord-95af83d0ea804de080ec944433f42fda
Source dataset
uspto-grants-1983_10
Patent number
US04407823

Reaction notes

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