HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 13576487, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Ethyl 4-[4-(4-trifluoromethylphenoxy)phenoxy]-3-hydroxypentanoate | HCID 12856783 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 13576487 | HCID 13576487 | — |
Reaction Steps
Ethyl 4-[4-(4-trifluoromethylphenoxy)phenoxy]-3-hydroxypentanoate is reacted with 1.1 equivalent of acetyl chloride and 1.0 equivalent of pyridine in benzene to yield ethyl 4-[4-(4-trifluoromethylphenoxy)phenoxy]-3-acetoxypentanoate. Similarly, using n-propanoyl chloride and isopropanoyl chloride yield the respective 3-n-propanate and 3-isopropanoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04408076 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-158d172b396441b9bd54012b1a99d832 |
| Source note | uspto-grants-1983_10 |