HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178490397, compound → BENZYL ALCOHOL, o-(5-(m-METHOXYPHENYL)-s-TRIAZOL-3-YL)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178490397 | HCID 178490397 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | BENZYL ALCOHOL, o-(5-(m-METHOXYPHENYL)-s-TRIAZOL-3-YL)- | HCID 53228 | — |
Reaction Steps
A suspension of 16 g of 4-[2-(3-methoxybenzyliden)hydrazino]-1H-2,3-benzoxazine in 160 cc of anhydrous xylene is refluxed for 45 minutes and then, cooled in an ice bath. The solid which precipitates is recovered by filtration and recrystallized from ethanol yielding 14.7 g of the compound of the title. M.p. 157°-59° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04409388 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-7d8462bd23b44b4ab9a60edb9bfd093f |
| Source note | uspto-grants-1983_10 |