HuagongsheHuagongshe Chemistry Print Report · For research reference only
Picolyl chloride → 2-{[(2-Ethyl-1,7-dioxaspiro[4.5]decan-2-yl)methoxy]methyl}pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Picolyl chloride | HCID 23393 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | (2-Ethyl-1,7-dioxaspiro[4.5]decan-2-yl)methanol | HCID 13237156 | — |
| Product | 2-{[(2-Ethyl-1,7-dioxaspiro[4.5]decan-2-yl)methoxy]methyl}pyridine | HCID 13237158 | — |
Reaction Steps
Following procedures similar to Embodiments I-V above, 2-ethyl-1,7-dioxaspiro[4.5]decane-2-methanol was treated with 2-picolinyl chloride in the presence of sodium hydride to yield the desired product as a pale amber oil, b.p. 123° C. (0.006 mm).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04410354 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-ca1fd97a99e84d0c9105279dab822005 |
| Source note | uspto-grants-1983_10 |