Sodium borohydride → HCID 178492594, compound

Participants

Reaction Steps

In this example, 848 mg of the product obtained in Example 7 is dissolved in 30 ml of ethanol. The solution is subjected to reaction in the same conditions as those of Example 6 by using 1 g of sodium borohydride. The reaction mixture is subjected to the same post-treatment as that of Example 6 to obtain crude crystals. The crude crystals are recrystallized from methanol to obtain 554 mg of the desired product.

Provenance & Evidence