HCID 20484393, compound → HCID 20484361, compound

HRID 647837Notes

Reaction equation

HRID 647837 reaction equation
[CH3:1][N:2]1[CH:6]([C:7](=[O:22])[C:8]2[CH:13]=[CH:12][C:11]([O:14]CC3C=CC=CC=3)=[CH:10][CH:9]=2)[CH:5]([CH2:23][CH2:24][CH3:25])[N:4]([CH3:26])[C:3]1=[O:27].[H][H]>C(O)C>[CH3:1][N:2]1[CH:6]([C:7](=[O:22])[C:8]2[CH:9]=[CH:10][C:11]([OH:14])=[CH:12][CH:13]=2)[CH:5]([CH2:23][CH2:24][CH3:25])[N:4]([CH3:26])[C:3]1=[O:27]

Participants

4

Reactant 2

HCID 20484393HCID 20484393, compoundHCID 178418361HCID 178418361, compound

Product 1

HCID 20484361HCID 20484361, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

1,3-dimethyl-4-propyl-5-(4-benzyloxybenzoyl)-2-imidazolidinone (10 g) is dissolved in 100 ml ethanol and the reaction flask charged with 100 mg 10% pallidium on charcoal. The mixture is hydrogenated at atmospheric pressure until 1 equivalent of hydrogen is consumed. After filtration and evaporation of solvent the title compound is obtained.

Workup

  1. additionthe reaction flask charged with 100 mg 10% pallidium on charcoal
  2. customis consumed
  3. filtrationAfter filtration and evaporation of solvent the title compound
  4. customis obtained

Sources & evidence

ORD record
ord-d92cea468b054adfa6e8adceb703bb1d
Source dataset
uspto-grants-1983_10
Patent number
US04410540

Reaction notes

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