HRID647899

反应详情

EQUATION

反应方程式

HRID 647899 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 5-(2-formyl-3-benzyloxyphenoxy) pentanoic acid (1.0 g, 0.003 M) in ethanol containing 5% palladium on charcoal catalyst (0.61 g) was hydrogenated at atmospheric pressure. After 20 minutes the reaction was complete and the catalyst was filtered off and the ethanol removed in vacuo to give 5-(2-formyl-3-hydroxyphenoxy)pentanoic acid, m.p. 94° C.

WORKUP

后处理

  1. filtrationthe catalyst was filtered off
  2. customthe ethanol removed in vacuo