HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → HCID 20484306, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | HCID 14715970 | HCID 14715970 | — |
| Product | HCID 20484306 | HCID 20484306 | — |
Reaction Steps
133 g of 2-chlorovalerophenone are added dropwise to 715 ml of fuming HNO3 at -15° C. and the mixture is poured onto 4 kg of ice. The aqueous phase is then extracted with chloroform and the organic phase is washed, dried and concentrated. The oily compound is further processed as the crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04410536 |
| Source dataset | uspto-grants-1983_10 |
| ORD ID | ord-f5318ac2148b4451a079ec620cfde4db |
| Source note | uspto-grants-1983_10 |