Piperonylamine → HCID 20484334, compound

HRID 647938Notes

Reaction equation

HRID 647938 reaction equation
Cl.[CH2:2]([C:6]1[C:10]2[CH:11]=[C:12]([NH:15]N)[CH:13]=[CH:14][C:9]=2[S:8][CH:7]=1)[CH2:3][CH2:4][CH3:5].O.Cl.[NH:19]1[CH2:24][CH2:23][C:22](=O)[CH2:21][CH2:20]1>>[CH2:2]([C:6]1[C:10]2=[C:11]3[C:12](=[CH:13][CH:14]=[C:9]2[S:8][CH:7]=1)[NH:15][C:22]1[CH2:23][CH2:24][NH:19][CH2:20][C:21]3=1)[CH2:3][CH2:4][CH3:5]

Participants

3

Reactant 2

HCID 2723901PiperonylamineHCID 20484281HCID 20484281, compound

Product 1

HCID 20484334HCID 20484334, compound

Procedure

The compound is formed analogously to that described in Example 15, from 25.6 g of 3-butyl-5-hydrazinobenzothiophene hydrochloride and 20 g of 4-piperidone hydrochloride monohydrate. Melting point: 224°-225° C.

Workup

  1. customThe compound is formed analogously to that

Sources & evidence

ORD record
ord-b18ca5fd9a8448e3b2c87b9a996cc7f8
Source dataset
uspto-grants-1983_10
Patent number
US04410536

Reaction notes

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