1-(Isopropyl)-4-piperidone → HCID 20484285, compound
Reaction equation
Cl.[CH2:2]([C:6]1[C:10]2[CH:11]=[C:12]([NH:15]N)[CH:13]=[CH:14][C:9]=2[S:8][CH:7]=1)[CH2:3][CH2:4][CH3:5].[CH:17]([N:20]1[CH2:25][CH2:24][C:23](=O)[CH2:22][CH2:21]1)([CH3:19])[CH3:18]>>[CH2:2]([C:6]1[C:10]2=[C:11]3[C:12](=[CH:13][CH:14]=[C:9]2[S:8][CH:7]=1)[NH:15][C:23]1[CH2:24][CH2:25][N:20]([CH:17]([CH3:19])[CH3:18])[CH2:21][C:22]3=1)[CH2:3][CH2:4][CH3:5]Participants
3
Procedure
The compound is formed analogously to that described in Example 15, from 25.6 g of 3-butyl-5-hydrazinobenzothiophene hydrochloride and 17 g of 1-isopropyl-4-piperidone. Melting point: 157°-158° C.
Workup
- customThe compound is formed analogously to that
Sources & evidence
- ORD record
- ord-9059643bb6db42ba9e9a608d3e399dbe
- Source dataset
- uspto-grants-1983_10
- Patent number
- US04410536
Reaction notes
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